Nanoscale reconstruction of surface crystallography from three-dimensional polarization distribution in ferroelectric barium-titanate ceramics

Publikation: Beitrag in FachzeitschriftForschungsartikelBeigetragenBegutachtung

Beitragende

  • L. M. Eng - , Professur für Experimentalphysik/Photophysik (Autor:in)
  • H. J. Güntherodt - , Universität Basel (Autor:in)
  • G. A. Schneider - , Technische Universität Hamburg (Autor:in)
  • U. Köpke - , Technische Universität Hamburg (Autor:in)
  • J. Muñoz Saldaña - , Technische Universität Hamburg (Autor:in)

Abstract

The three-dimensional orientation of polarization vectors at the surface of ferroelectric barium-titanate (BaTiO3) ceramics is evaluated using voltage-modulated scanning force microscopy (SFM). By applying an ac voltage to the conductive SFM tip, we measure the relative amount of the three orthogonal components Px, Py, and Pz, of the polarization vector at any surface point. The measured polarization orientation together with the actual domain-wall orientation allows a precise reconstruction of the crystallographic orientation of the investigated grains down to a 40 nm resolution. Excellent agreement is obtained when comparing this orientation with the crystallographic reconstruction revealed by etch patterns from the sample surface topography. We show that the surface topography manifests a domain structure, which was present in the past, while the actual ferroelectric domain configuration is revealed by the modulation technique.

Details

OriginalspracheEnglisch
Seiten (von - bis)233-235
Seitenumfang3
FachzeitschriftApplied physics letters
Jahrgang74
Ausgabenummer2
PublikationsstatusVeröffentlicht - 11 Jan. 1999
Peer-Review-StatusJa

Externe IDs

ORCID /0000-0002-2484-4158/work/158768112

Schlagworte

ASJC Scopus Sachgebiete