Intergrowth of several solid phases from the Y-Ni-B-C system in a large YNi2B2C crystal

Publikation: Beitrag in FachzeitschriftForschungsartikelBeigetragenBegutachtung

Beitragende

  • Torsten Weissbach - , Technische Universität Dresden (Autor:in)
  • Tilmann Leisegang - , Technische Universität Dresden (Autor:in)
  • Andreas Kreyssig - , Technische Universität Dresden, Ames Laboratory (Autor:in)
  • Matthias Frontzek - , Technische Universität Dresden (Autor:in)
  • Jens Uwe Hoffmann - , Helmholtz-Zentrum Berlin für Materialien und Energie (HZB) (Autor:in)
  • Dmitri Souptel - , Leibniz Institute for Solid State and Materials Research Dresden (Autor:in)
  • Anke Köhler - , Leibniz Institute for Solid State and Materials Research Dresden (Autor:in)
  • Günter Behr - , Leibniz Institute for Solid State and Materials Research Dresden (Autor:in)
  • Peter Paufler - , Institut für Strukturphysik (ISP1), Institut für Festkörper- und Materialphysik (Autor:in)
  • Dirk C. Meyer - , Juniorprofessur für Nanostrukturphysik (Autor:in)

Abstract

A YNi2B2C single crystal containing traces of foreign phases was inspected by means of neutron and X-ray diffraction as well as scanning electron microscopy and X-ray spectroscopy methods. The diffraction patterns obtained from the experiments look similar to those expected for a superstructure. Nevertheless, they can be interpreted as crystallographically oriented precipitations of YB2C2 and Ni2B within the YNi2B2C crystal, formed during the cooling process. The orientation relation between the lattices was obtained from experimental neutron and X-ray data. Structure refinements of the collected X-ray data were performed by separation of the intensity data of the individual phases. Scanning electron microscopy images of the inclusions found on a polished cross section of the crystal are presented; their chemical composition was determined using wavelength-dispersive X-ray analysis.

Details

OriginalspracheEnglisch
Seiten (von - bis)738-746
Seitenumfang9
FachzeitschriftJournal of applied crystallography
Jahrgang41
Ausgabenummer4
PublikationsstatusVeröffentlicht - 2008
Peer-Review-StatusJa

Schlagworte

Schlagwörter

  • Intermetallic compounds, Single-crystal diffraction methods