Survey on Methodes for Analysis and Conservation of Hydrated Lime Particles Sampled in Flue Gas Cleaning Systems

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Abstract

In terms of analyzing and modeling conditioned dry
absorption, an unbiased view on the injected hydrated lime particles is
needed. Multiple investigations on the reaction mechanisms are reported in
the literature. Nevertheless, outstanding issues still exist as a necessary
conservation in the time between the particle sampling and analysis as well as
the suitability of the analyzing methods itself has been regarded only roughly
yet. Thus, in this work TGA, XRD, and SEM-EDS were used for analyzing
Ca(OH)2-CaCl2·2H2O-mixtures. TGA turned out to be inappropriate as the
composition of the mixture changes during analysis. A cooling of the particle
samples down to 277.15 K under air exclusion proved to be a sufficient
conservation method for the time span between sampling and analysis.

Details

Original languageEnglish
Number of pages7
JournalIndustrial & Engineering Chemistry Research
Volume57
Issue number6
Publication statusPublished - 2018
Peer-reviewedYes

Keywords

Subject groups, research areas, subject areas according to Destatis

Keywords

  • Analysis, Hydratet Lime Particles, Conservation, Flue Gas Cleaning Systems