Miniaturised test-setup for Spark Plasma Sintering - experimental and numerical investigations

Research output: Contribution to journalResearch articleContributedpeer-review

Contributors

Abstract

Spark Plasma Sintering (SPS) is an innovative sintering technique, whereby many of the beneficial effects of this process on sintering are still elusive. To allow for the detailed investigations of the SPS process, a custom experimental set-up and a corresponding finite element (FE) model was developed. The miniaturised setup allows for very high current intensities, custom pulse patterns, a wide pressure range and dilatometric measurements. The FE model was employed to calculate the temperature field in the set-up and the sintering specimen itself. A very good correlation of the temperature, current and voltage over the entire process was observed. Our investigations show that the contact conductivities have a significant impact on the process temperature. Also, the imperfect contacts at the interfaces between the graphite foil and the real specimen may lead to a significant variance of the currents necessary to obtain the desired sintering temperature.

Details

Original languageEnglish
Pages (from-to)461 - 471
Number of pages11
JournalPowder Metallurgy
Volume66
Issue number5
Publication statusPublished - 2023
Peer-reviewedYes

External IDs

Scopus 85161944776

Keywords