Bending tests of delignified and densified poplar

Research output: Contribution to journalResearch articleContributedpeer-review

Abstract

Wood modification has a long tradition to improve durability and other properties. In this study, a combination of delignification and densification to enhance bending strength and ASE (antiswelling efficiency) was introduced. Both treatments change the properties of modified wood in different ways depending on the conditions and species. The objective of this treatment combination was the improvement of mechanical properties by partly extracting lignin. The treated structure retains the alignment of cellulose and hemicellulose chains. The densification perpendicular to the grain reduced the cell lumina and compressed the wood structure by more than 70%. As a result, the cell walls become decreased entangled and new hydrogen bonds between adjacent cellulose nanofibres were linked. The combined processes were applied to the green and dried poplar (Populus nigra L.). Firstly: the delignification procedure was done with small specimens in NaOH and Na2SO3 solution at 100 degrees C, 130 degrees C or 150 degrees C for 7 h. After washing and analysing wood components densification followed. The wood was compressed 80% perpendicular to the grain in different temperatures (100 degrees C, 130 degrees C, 160 degrees C) and pressing times (4, 20, 24 h) of the original thickness. After the treatment, ASE and bending strength (MoR, MoE) were determined. The bending strength was meanly dependent on the solution temperature and compression time and temperature. Bending strength will increase up to 450 MPa and has the optimum at around 90% lignin removal and 130 degrees C pressing time over 24 h. ASE was reduced by strong delignification and increasing temperature.

Details

Original languageEnglish
Pages (from-to)42-50
Number of pages9
JournalWood material science & engineering
Volume18
Issue number1
Early online dateOct 2022
Publication statusPublished - 2 Jan 2023
Peer-reviewedYes

External IDs

Scopus 85141195272
ORCID /0000-0002-5948-2097/work/168207461

Keywords

ASJC Scopus subject areas

Keywords

  • Bending strength, delignification, densification, poplar, swelling