The Dresden in-situ (S)TEM special with a continuous-flow liquid-helium cryostat

Publikation: Beitrag in FachzeitschriftForschungsartikelBeigetragenBegutachtung

Beitragende

Abstract

Fundamental solid state physics phenomena often occur at very low temperatures, requiring liquid helium cooling in experimental studies. Transmission electron microscopy is a well-established characterization method, which allows probing crucial materials properties down to nanometre and even atomic resolution. Due to the limited space in the object plane, however, suitable liquid-helium cooling is very challenging. To overcome this limitation, resolving power was sacrificed in our Dresden in-situ (S)TEM special, resulting in more than 60 mm usable experimental space in all directions with the specimen in the centre. With the installation of a continuous-flow liquid-helium cryostat, any temperature between 6.5 K and 400 K can be set precisely and kept for days. The information limit of the Dresden in-situ (S)TEM special is about 5 nm. It is shown that the resolution of the Dresden in-situ (S)TEM special is currently not limited by aberrations, but by external instabilities.

Details

OriginalspracheEnglisch
Seiten (von - bis)12-20
Seitenumfang9
FachzeitschriftUltramicroscopy
Jahrgang203
PublikationsstatusVeröffentlicht - Aug. 2019
Peer-Review-StatusJa

Externe IDs

PubMed 30902417

Schlagworte

Schlagwörter

  • In-situ, Instrumentation, STEM, TEM